Glossary
4He Can
Also known as helium bath. Used to store helium.
Helium gets in through the transfer tube
and exits through the exhaust port, cooling the
aluminum shield via the copper plate.
Helium is also drawn into the 1K pot through the feed capillary,
continuous fill capillary
and single-shot valve. The bottom of the can has the connection for
the thermal link to the
sorption pump, miniflange connector to the feed capillary
and mount for the IVC tail.
Superinsulation
Thin aluminized mylar. Used to cover the IVC and the aluminum
shield to cut on the radiation
heat leak and heat transfer due to hot molecules.
IVC Neck
In order to reduce the heat leak via thermal conductivity along
the walls of the IVC, the
top part of it ("neck") has a folded structure. Effectively,
the length of this segment
is increased by a factor of 3.
Windows
Windows in the outer dewar and the IVC are made of Kapton.
Beryllium is used for
the cell windows. The aluminum shield has thin aluminum foil
instead of the windows in
order to cut down on infrared radiation from the room to the cell.
Cell
The experimental cell, or the sample chamber, consists of two major parts:
the body and
the lid. The body is just a piece of copper with beryllium windows
put into it.
The lid has the sample holder and the voltage bias electrode
attached from the inside;
and the pressure gauge, the sample valve and an indium seal
miniflange connector
from the outside. The lid and the body are screwed together
with an indium
gasket between them.
Exhaust Port
Helium exhaust from the helium bath exits here.
Aluminum Shield
The aluminum radiation shield stays at a temperature
between that of the helium bath (4 K) and the outer dewar wall (300 K).
Its purpose is to intercept radiation flux coming
from the outer wall,
and to capture hot molecules of the
residual gas desorbing from it. It is being cooled
by the exiting helium boil-off gas through the top copper plate
to which it is attached with a set of screws. The aluminum shield is
wrapped around with ~50 layers of superinsulation.
Outer Vacuum Chamber (OVC)
The outer vacuum chamber is a name for the vacuum volume separating
the IVC and the helium bath from the outer dewar wall. It has to be
pumped out (through the pump ports) to low pressure (less than 10^(-7)
torr) in order to reduce
heat exchange via thermal conductivity through the gas. The aluminum shield
does not separate two different vacui. The pressure in the OVC is monitored
by Pirani and Penning pressure gauges.
Outer Dewar Wall and Lid
The most visible part of the cryostat. It separates the OVC from the outside
world. In the lower part it has Kapton X-Ray windows, and the mounting support
for attaching the cryostat to the Huber goniometer. The top lid of the outside
container has the suspension system attached to it. There is a pump port and
two pressure gauge ports on the outer wall; and electronics feed-throughs,
helium transfer port and the helium exhaust port on the top lid of the
dewar.
Pump and Pressure Gauge Ports
The pump station connects to the pump port through flexible bellows.
Pirani and Penning pressure gauges connect to the pressure gauge ports.
Sorption Pump
The sorption pump is just a copper container with activated charcoal
inside. The charcoal releases almost all of the gas at temperatures above
about 35 K and absorbs gas almost perfectly below 10K.
Condenser
The condenser is a piece of copper tubing silver soldered into the 1K Pot. It
is connected to the sorption pump from the top and to the
3He Pot from the bottom. When the sorption pump is heated, the
gas condenses on the cold surface of the condenser and drips into the
3He Pot.
1K Pot
The 1K pot is a container in the IVC which under normal conditions runs
at about 1.3 K. Liquid 4He is drawn from the main helium bath
through the capillary and the single shot valve. Gasious He then escapes
through the pump plumbing and the exhaust port on top of the IVC.
3He Pot
The coldest point of the cryostat. The sorption pump pumps on the 3
He in it lowering its temperature. The sample cell connects to the copper plate
on which the 3He Pot is mounted.
Diode Thermometers
There are three diode thermometers in the cryostat. One of them is connected
to the sorption pump, and the other two are on the top and the bottom of the
aluminum shield.